化学
衍射仪
吸光度
粒径
扫描电子显微镜
Zeta电位
结晶度
柠檬酸钠
银纳米粒子
纳米颗粒
核化学
表征(材料科学)
动态光散射
分析化学(期刊)
化学工程
纳米技术
色谱法
结晶学
材料科学
晶体结构
物理化学
工程类
病理
医学
复合材料
作者
Prem Santhi Yerragopu,Sharanagouda Hiregoudar,Udaykumar Nidoni,K. T. Ramappa,A. G. Sreenivas,S. R. Doddagoudar
出处
期刊:International Research Journal of Pure and Applied Chemistry
[Sciencedomain International]
日期:2020-03-24
卷期号:: 37-50
被引量:37
标识
DOI:10.9734/irjpac/2020/v21i330159
摘要
The present work was aimed to study the synthesis of silver nanoparticles (Ag NPs) using Tri-Sodium Citrate (TSC), stability study of synthesized Ag NPs and their characterization. Synthesis of Ag NPs has been carried out by maintaining different conditions such as TSC concentration (0.50, 1.00 and 1.50%), AgNO3 concentration (0.50, 1.00 and 1.50 mM) and stirring time (10, 15 and 20 min). The stability study of synthesized Ag NPs conducted for 30 days without adding any stabilizing agents. The characterization of synthesized Ag NPs was carried out for different parameters like particle size and zeta potential using particle size analyzer, absorbance peak by UV-Visible spectrophotometer, morphology by Scanning Electron Microscope (SEM), crystallinity by X-Ray Diffractometer (XRD) and material structural characteristics by Atomic Force Microscope (AFM). The stable chemically synthesized Ag NPs were obtained at C20 (AgNO3 concentration of 1.5 mM, TSC 1.5% and stirring time 20 min) (desirability 99.97%), with average particle size of 22.14 nm and average absorbance peak of 449.85 nm.
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