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Mg2+/Li+ separation by electric field assisted nanofiltration:the impacts of membrane pore structure, electric property and other process parameters

电场 纳滤 化学工程 化学 过程(计算) 材料科学 计算机科学 工程类 生物化学 量子力学 操作系统 物理
作者
Quan Li,Yahui Liu,Yanghe Liu,Yanhong Ji,Zhenyu Cui,Yan Feng,Jianxin Li,Mohammad Younas,Benqiao He
出处
期刊:Journal of Membrane Science [Elsevier]
卷期号:662: 120982-120982 被引量:12
标识
DOI:10.1016/j.memsci.2022.120982
摘要

An electric field assisted nanofiltration (ENF) process was used for Mg 2+ /Li + efficient separation from a MgCl 2 /LiCl solution and a simulated salt-lake brine. The influence of membrane pore structure, electric property, and other process parameters on the Mg 2+ /Li + separation performance in the ENF was systematically investigated. The structural coefficient ( λ ) of NF membrane was introduced to quantify the membrane pore structure including pore size, pore length and porosity. Results suggested that membrane pore structure, instead of membrane pore size, had a critical role on the ENF separation performance. Direct current electric field (DC-EF) markedly promoted Mg 2+ /Li + separation. However, the effect of alternating current EF (AC-EF) with different frequencies was nominal. The synergistic effect between λ and DC-EF on Mg 2+ /Li + separation was also demonstrated. A low-concentration feed with suitable Mg 2+ /Li + mass ratio and pH value, and low transmembrane pressure were beneficial to Mg 2+ /Li + separation. For 2000 ppm MgCl 2 /LiCl feed solution with a Mg 2+ /Li + mass ratio of 20, a nearly complete rejection to Mg 2+ and a high Li + flux simultaneously achieved; correspondingly, a separation factor of Li + over Mg 2+ ( S Li,Mg ) reached above 7000, which is 2-3 orders of magnitude higher than that of pure NF membrane. For a simulated 10,000 ppm brine solution, a S Li,Mg value was up to above 50. The study suggested that ENF process witnessed simple and efficient separation performance for Li + extraction from salt lakes. • The electric-field assisted nanofiltration (ENF) process had an ultra-high Mg 2+ /Li + separation performance. • The structural coefficient ( λ ) of NF membrane played a key role in the ENF process. • Direct current electric field (DC-EF) markedly promoted Mg 2+ /Li + separation. • There was a synergistic effect between DC-EF and λ on Mg 2+ /Li + separation.
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