New insights into ductility improvement of a nickel-based superalloy through grain boundary engineering

Grain boundary engineering (GBE) provides an effective approach for tailoring the properties of metallic materials by optimizing the grain boundary character distribution (GBCD). Using electron backscatter diffraction analysis and uniaxial tensile testing at room temperature, this study systematically investigated the impact of GBE-type thermomechanical processing (TMP) on the ductility of an Incoloy 925 nickel-based superalloy (Alloy 925). The results showed that at 5 % strain, increasing the annealing temperature results in larger twin-related domains through strain-induced boundary migration. The GBE-type TMP can significantly enhance the ductility of Alloy 925, namely, the elongation increases from 64.22 % to 95.86 % as the annealing temperature increases from 1050 °C to 1100 °C. The evolved GBCD introduces more coherent twin boundaries with lower average residual Burgers vectors, enabling efficient dislocation transmission. In addition, extensive twinning can widely generate some soft orientations and simultaneously reduce the average Taylor factor within the twin clusters, leading to easy dislocation activation during plastic deformation. The synergistic effect of the optimized grain boundary network and twin cluster anisotropy promotes uniform plastic flow and effective strain accommodation, thereby enhancing the ductility of Alloy 925. Overall, this work provides novel and valuable insights into ductility optimization through GBE in a nickel-based superalloy.