Synthesis of silver nanoparticles by atmospheric pressure plasma jet

银纳米粒子 材料科学 硝酸银 柠檬酸三钠 纳米颗粒 表面等离子共振 动态光散射 大气压等离子体 化学工程 拉曼散射 大气压力 透射电子显微镜 纳米材料 纳米技术 拉曼光谱 分析化学(期刊) 等离子体 光学 有机化学 化学 工程类 地质学 物理 海洋学 量子力学
作者
Tatiana Habib,José Maurício A. Caiut,Bruno Caillier
出处
期刊:Nanotechnology [IOP Publishing]
卷期号:33 (32): 325603-325603 被引量:17
标识
DOI:10.1088/1361-6528/ac6528
摘要

Silver nanoparticles are one of the most extensively used metallic nanomaterials due to their unusual physical and chemical properties as well as their promising applications in a wide range of different fields. In this study, a non-thermal atmospheric pressure helium plasma jet was used to successfully synthesize silver nanoparticles with silver nitrate as a precursor and trisodium citrate as a capping agent. The browning of the solution after only 5 min of plasma irradiation is a result of the surface plasmon resonance (SPR) from the obtained silver nanoparticles. The SPR was confirmed by the presence of an absorption band in the visible range between 400 and 450 nm demonstrated in the UV-vis spectra. The effect of different chemical parameters such as the concentration of silver nitrate and the concentration of citrate on the silver nanoparticles have been studied. These nanoparticles were further characterized using transmission electron microscopy and dynamic light scattering. Therefore, the plasma jet was advantageous to fast produce silver nanoparticles in friendly conditions. In addition, the used experimental setup allows further studies in different solvents conditions and with different capping agents. So, this methodology could be useful for the preparation of silver nanoparticles required for numerous applications such as bioactivity, catalysis, surface enhanced Raman scattering, and photonic.
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