Microstructural damage characterization of concrete under freeze-thaw action

This paper conducts a quantitative analysis of microstructural damage evolution of concrete materials under freeze-thaw action using three-dimensional X-ray computed tomography. The study employs two resolution-scales to evaluate concrete samples under various cycles of freeze-thaw action. The three-dimensional microstructural damage characterization, pore network (porosity, pore size, and pore distribution) as well as the defects in the aggregates are specifically investigated. The microstructures of concrete under different freeze-thaw action show that the interfacial transition zone is most likely to be damaged first under frost attack. Furthermore, the freeze-thaw action deteriorates not only the interfacial transition zone but also cement matrix and aggregates. The impact of freeze-thaw cycles is notable on the internal micro-pores and micro-cracks of the concrete. More pores and cracks can be nucleated during the freeze-thaw action, and further accumulate and grow in the paste and aggregates, eventually leading to final failure of concrete materials. As demonstrated in this study, three-dimensional X-ray computed tomography is capable of acquiring microstructures of concrete and revealing existence of internal pores and cracks in different phases of concrete, and more effective to characterize accumulated damage of concrete due to freeze-thaw action.