起爆
元素分析
标准生成焓
碳-13核磁共振
化学
衍射
单晶
核磁共振波谱
光谱学
材料科学
分析化学(期刊)
物理化学
结晶学
有机化学
爆炸物
光学
物理
量子力学
作者
Chunlin He,Jiaheng Zhang,Damon A. Parrish,Jean’ne M. Shreeve
出处
期刊:Journal of materials chemistry. A, Materials for energy and sustainability
[The Royal Society of Chemistry]
日期:2013-01-01
卷期号:1 (8): 2863-2863
被引量:103
摘要
A series of 3,5-dinitropyrazole derivatives was prepared from 4-chloro-3,5-dinitropyrazole in good yields and characterized by IR, 1H, and 13C NMR (some cases 15N NMR) spectroscopy, elemental analysis, and DSC. The structures of 7 and 13 were confirmed by single crystal X-ray diffraction. The impact sensitivity was determined using a standard BAM method, and detonation properties were obtained using experimental densities and calculated heats of formation.
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