葡聚糖
化学
硅胶
柱色谱法
辛烷值
色谱法
乙酸乙酯
化学成分
皮质(解剖学)
化学结构
立体化学
有机化学
生物
酶
神经科学
作者
Yan‐Qun Liu,Yang Sheng-hui,Qiang Liu,Gang Pei,Wei-wei Pan,Min Liu,Caiyun Peng
出处
期刊:PubMed
日期:2013-11-01
卷期号:36 (11): 1792-5
被引量:3
摘要
To study the chemical constituents of Zanthoxyli Cortex.The chemical constituents were isolated and purified by silica gel and HP-20, MCI gel, Sephadex LH -20 column chromatography, RP-18 and PTLC. Their structures were elucidated by the analysis of spectral data and chemical properties.Ten compounds were isolated from EtOAc extract and their structures were identified as: asarinin (I), fargesin (II), eudesmin (III), (1R, 2R, 5R, 6S)-2-(3,4-dimethoxyphenyl)-6-(3,4-dihydroxyphenyl)-3,7-dioxabicyclo[3.3.0]-octane(IV), dimethoxysamin(V), rel-(1R,5R,6S)-6-(3,4-dimethoxyphen-yl)-3,7-dioxabicyclo-[3.3.0]-octan-2-one(VI), Magnone A(VII), beta-sitoste-rol( VIII), beta-armyrin(IX), beta-amyrone(X).These compounds isolated from Zanthoxyli Cortex's Ethyl acetate extract are all known compounds. Fargesin(II) and beta-amyrone(X) are isolated from Zanthoxyli Cortex for the first time.
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