钇
热重分析
插层(化学)
氢氧化物
电化学
氧化物
无机化学
材料科学
扫描电子显微镜
盐(化学)
化学工程
水溶液
沉积(地质)
核化学
化学
冶金
电极
物理化学
复合材料
古生物学
沉积物
工程类
生物
作者
Igor Zhitomirsky,Anthony Petric
摘要
Thin films of yttrium hydroxide were obtained from aqueous Y(NO3)3 and YCl3 salt solutions via cathodic electrodeposition. The electrodeposition yield was studied under various experimental conditions. By varying the current density, deposition time and yttrium salt concentration, the amount of the deposited material could be controlled. Electrochemical intercalation of poly(diallyldimethylammonium chloride) into the hydroxide deposits has been demonstrated and the mechanism of intercalation has been discussed. The deposits were studied by X-ray diffraction, thermogravimetric analysis and scanning electron microscopy. Formation of crystalline yttrium oxide films from the hydroxide precursor was observed at 600 °C.
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