材料科学
热重分析
钻井液
化学工程
热稳定性
水溶液
吸水率
过硫酸铵
复合材料
聚乙烯醇
聚合物
单体
化学
有机化学
钻探
冶金
工程类
作者
Peng Xu,Jun Yu,Lingzhi Xie
出处
期刊:Polymers
[MDPI AG]
日期:2024-06-11
卷期号:16 (12): 1658-1658
标识
DOI:10.3390/polym16121658
摘要
Gel plugging agents have become one of the preferred methods for plugging in complex and severe loss conditions during drilling due to their good adaptability to loss channels. To address the common issue of poor temperature resistance in gel-based plugging agents, high-temperature-resistant gel plugging materials were synthesized through the molecular design of polymers, modifying existing agents. Based on the temperature and salt resistance of the aqueous solution of an acrylamide (AM)/N-vinylpyrrolidone (NVP) binary copolymer, temperature-resistant monomer sodium styrene sulfonate (SSS) was introduced and reacted in a polyvinyl alcohol (PVA) aqueous solution. Using ammonium persulfate (APS) as an initiator and crosslinking with N,N-methylenebisacrylamide (MBA), a gel plugging material resistant to 140 °C was synthesized. The structure, thermal stability, water absorption and expansion, and plugging performance of the gel were studied through hot rolling aging, thermogravimetric analysis, infrared spectroscopy, electron microscopy scanning, sand bed experiments, and drag reduction experiments. The results show that the gel material has good thermal stability and water absorption and expansion at 140 °C, and its temperature-resistant plugging performance is excellent, significantly slowing down the loss rate of drilling fluid. This provides a basis for the further development of gel materials.
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