微流控
模块化设计
循环伏安法
化学
纳米技术
吞吐量
电化学
电极
阳极
组合化学
材料科学
计算机科学
电信
物理化学
无线
操作系统
作者
Yiming Mo,Girish Rughoobur,Anirudh M. K. Nambiar,Kara Zhang,Klavs F. Jensen
标识
DOI:10.1002/ange.202009819
摘要
Abstract Electroorganic synthesis is a promising tool to design sustainable transformations and discover new reactivities. However, the added setup complexity caused by electrodes in the system impedes efficient screening of reaction conditions. Herein, we present a microfluidic platform that enables automated high‐throughput experimentation (HTE) for electroorganic synthesis at a 15‐microliter scale. Two HTE modules are demonstrated: 1) the rapid electrochemical reaction condition screening for a radical–radical cross‐coupling reaction on micro‐fabricated interdigitated electrodes, and 2) measurements of kinetics for mediated anodic oxidations using the microliter‐scale cyclic voltammetry. The presented modular approach could be deployed for a range of other electroorganic chemistry applications beyond the demonstrated functionalities.
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