萃取(化学)
采样(信号处理)
复矩阵
基质(化学分析)
杀虫剂
生物累积
样品制备
色谱法
生化工程
环境化学
化学
环境科学
土工试验
计算机科学
检出限
土壤水分
生物
生态学
土壤科学
工程类
滤波器(信号处理)
计算机视觉
作者
Ahmad Husaini Mohamed,Nur Athirah Noorhisham,Noorfatimah Yahaya,Sharifah Mohamad,S. Kamaruzzaman,Hasnah Osman,Hassan Y. Aboul‐Enein
标识
DOI:10.1080/10408347.2021.1992262
摘要
Despite organophosphorus pesticides (OPPs) benefits in controlling vector-borne diseases and noxious insects, the bioaccumulation and persistence in the soil system may metamorphose into new substances which could pose a serious threat to the ecosystems and human health. The generally low levels of OPPs residues and often the complexity of the soil matrix are the issues that researcher must deal with. Thus, it is essential to isolate and preconcentrate the OPPs from the matrix to reduce interference effects to obtain a reliable detection. Researchers have reported sample preparation techniques as a promising approach to improve analytical measurement of merits including recovery, precision, linearity, limit of detection, and limit of quantification. Under the selected conditions, limits of detection range between 0.001 and 143 ng/mL, and extraction recovery range between 5 and 154% were obtained. This review evaluates the challenges and opportunities, emphasizes the prospects of sampling techniques and various (micro)extraction coupled with chromatographic methods in different soil samples. Based on the finding, the extraction efficiency depended largely on the interaction between OPPs and extraction media. The fate, migration, toxicity impact, sampling procedure, and storage which influenced the sample preparation were comprehensively discussed.
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