纳米棒
扫描电子显微镜
材料科学
光致发光
傅里叶变换红外光谱
水溶液
化学工程
光谱学
微量分析
红外光谱学
分析化学(期刊)
能量色散X射线光谱学
表征(材料科学)
核化学
纳米技术
化学
物理化学
有机化学
复合材料
光电子学
工程类
物理
量子力学
作者
Ghazal Kianpour,Masoud Salavati‐Niasari,Hamid Emadi
标识
DOI:10.1016/j.ultsonch.2012.08.012
摘要
NiMoO(4) nanorods have been successfully synthesized by sonochemical method process by using Ni(CH(3)COO)(2) · 4H(2)O and (NH(4))(6)Mo(7)O(24) · 4H(2)O as starting materials. Some parameters including ultrasonic power, ultrasonic irradiation time, stirring effect, solvent effect, and surfactant effect were investigated to reach optimum condition. The as synthesized nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmittance electron microscopy (TEM), photoluminescence (PL) spectroscopy, Fourier transform infrared (FT-IR) spectra and energy dispersive X-ray microanalysis (EDX). Facile preparation and separation are important features of this route. This work has provided a general, simple, and effective method to control the composition and morphology of NiMoO(4) in aqueous solution, which will be important for inorganic synthesis methodology.
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