X射线光电子能谱
衍射仪
材料科学
透射电子显微镜
六方晶系
化学工程
纳米晶
结晶学
核化学
分析化学(期刊)
纳米技术
化学
晶体结构
有机化学
工程类
作者
Hua Lin,Bo Tang,Qing Li,Yanrong Li
出处
期刊:Advanced Materials Research
日期:2011-02-21
卷期号:194-196: 660-664
被引量:9
标识
DOI:10.4028/www.scientific.net/amr.194-196.660
摘要
V 2 O 3 and VN nanocrystals have been conveniently synthesized from thermal ammonolysis of the precursor VOC 2 O 4 •H 2 O in a resistance tubular furnace at 500°С and 780°С for 30 min, respectively. The products were characterized by X-ray diffractometer (XRD)、X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM) techniques. The average particle sizes of V 2 O 3 and VN are both in the ranges of 20~35 nm. The evolution from precursor to hexagonal V 2 O 3 and then to cubic VN was explored. The crucial factors,such as the reaction temperature and time,have also been discussed.
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