萃取(化学)
响应面法
产量(工程)
色谱法
化学
原材料
超声波传感器
材料科学
有机化学
声学
物理
冶金
作者
Milad Hadidi,Albert Ibarz,Jordi Pagán
出处
期刊:Food Chemistry
[Elsevier]
日期:2019-11-06
卷期号:309: 125786-125786
被引量:61
标识
DOI:10.1016/j.foodchem.2019.125786
摘要
The ultrasonic-assisted extraction of total saponins from alfalfa leaves was optimised by the simultaneous maximization of the yield and bioaccessibility as a factor with increasingly great relevance in the biological activity by Response Surface Methodology. The kinetics of total saponins and bioaccessibility were investigated for the optimum ultrasound-assisted method compared to conventional method by the pseudo-first order model. The optimum extraction conditions were of solvent/raw material ratio of 11.4 mL/g, extraction time of 2.84 h, extraction temperature of 76.8 °C, ultrasound power of 112.0 w and ethanol concentration of 78.2%. The yield of total saponins and bioaccessibility was 1.61 and 18.6%, respectively. The yield rate constant for the ultrasound extraction was almost two times more than that of the heat-reflux method. Ultrasonic-assisted extraction, comparing to conventional method, had greater efficiency for the extraction yield and bioaccessibility of total saponins.
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